High energy density materials by Anthony J. Bellamy (auth.), T. M. Klapötke (eds.)

By Anthony J. Bellamy (auth.), T. M. Klapötke (eds.)

A.J. Bellamy: FOX-7 (1,1-Diamino-2,2-dinitroethene).-

R.P. Singh, H. Gao, D.T. Meshri, J.M. Shreeve: Nitrogen-Rich Heterocycles.-

T.M. Klapötke: New Nitrogen-Rich excessive Explosives.-

R.D. Chapman: natural Difluoramine Derivatives.-

B.M. Rice, E.F.C. Byrd, W.D. Mattson: Computational features of Nitrogen-Rich HEDMs.-

S. Zeman: Sensitivities of excessive power Compounds

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1,2,3- and 1,2,4-Triazolium Heterocycles . . . . . . Triazolium Heterocycles Containing Amino Substituents . Triazolium Heterocycles Containing Azido Substituents . . Triazolium Heterocycles Containing Fluoroalkyl Substituents 1,2,4-Triazoliun Azolate Heterocycles . . . . . . . . . . . . . . . . . . . 3 Tetrazolium-Based Heterocycles . . . . . . . . . . . Tetrazolium Heterocycles Containing Amino and Azido Substituents . Tetrazolium Heterocycles Containing 5,5 -Azotetrazolate Anions .

The heat of formation at 25 ◦ C was calculated to be + 218 kJ mol–1, 26 kJ mol–1 greater than that for RDX. 1,3-Dinitro-1,3-diazacyclobutane therefore contains considerably more energy than FOX-7 (– 113 kJ mol–1 ) and its other isomers (trans – 80 kJ mol–1, cis – 29 kJ mol–1 ). 28 kJ g–1 (experimental) for RDX]. Thus, from an energy release viewpoint 1,3-dinitro-1,3-diazacyclobutane would appear to be a worthwhile target molecule for synthesis. However it is most probable that FOX-7 (1,1-Diamino-2,2-dinitroethene) 27 Table 2 Measured and computed bond lengths, bond angles and crystallographic data of FOX-7 Bemm et al.

3 Tetrazolium-Based Heterocycles . . . . . . . . . . . Tetrazolium Heterocycles Containing Amino and Azido Substituents . Tetrazolium Heterocycles Containing 5,5 -Azotetrazolate Anions . . Bistetrazolate Heterocycles . . . . . . . . . . . . . . . . . . 52 52 56 60 4 Urotropinium-Based Heterocycles . . . . . . . . . . . . 63 5 Tetrazine-Based Heterocycles . . . . . . . . . . . . . 65 6 Azetidinium-Based Heterocycles . . . . . .

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