Advances in lipid methodology. / 4 by edited by William W. Christie, ....

By edited by William W. Christie, ....

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121. 122. 123. 124. 125. 126. 127. 128. 129. 130. 131. 132. 133. 134. 135. 136. 137. 138. 139. 140. 141. 142. 143. 144. 145. 146. 147. 148. 149. 150. 151. 152. 153. 154. 155. 156. ANALYSIS OF PLANT LIPOXYGENASE METABOLITES Wurzenberger,M. , Z. Lebensm. Unters. , 175, 186-190 (1982). J. , J. Biol. , 268, 1708-1715 (1993). -E. ,An:h. Biochem. , 277, 86-93 (1990). N. , 371, 159-162 (1995). A. , FEBS Lett. 280, 159162 (1991). , Anal. , 188, 38-47 (1990). Kaplan,E. , J. , 268, 435-443 ( 1985). A. , Biochemistry, 34, I 0538-10545 (1995).

Anal. ,65, 1843-1852(1993). , Pawliszyn,J. , Anal. , 64, 19601966 (1992). , Anal. , 69, 364-372 (1997). , Miyamoto,K. , J. , 658, 129-142 (1994). , Lipids, 26, 407-415 (1991). , Biochem. Biophys. Res. , 156, 543-550 (1988). C. , Lipids, 13, 313-315 (1978). A. , 75, 458-461 (1984). , 50, 324-325 (1972). Vioque,E. ,Arch. Biochem. , 99, 522-528 (1962). J. , Anal. , 213, 218"225 (1993); erratum Anal. , 216, 241 (1994). , Kajiwara,T. , Phytochemistry, 15, 1889-1891 (1976). , Kajiwara,T. , Agric. Biol.

They found that com AOS catalysed formation of 12-oxo-PDA with a preference for the 9S,13S side chains. It is now known that the preference was caused by the action of allene oxide cyclase [70]. The strategy used by Hamberg et al. [69] was to synthesise the fully saturated methyl 12R- and 12S-hydroxy-9S,13R-phytonoate from a precursor of known stereochemistry, (-)-jasmonic acid (through alkali isomerization of (+)-7-iso-jasmonic acid). The 12R-hydroxy epimer was identified as the most polar on 1LC based on prior work showing that a trans relationship between the C-12 hydroxyl and C-13 side-chain results in the most polar epimer relative to the cis.

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